TECHNICAL BULLETIN
Preparing Concrete Slab
The most difficult aspect of satisfactorily coating a concrete floor is preparing the floor to ensure the
coating system will adhere. The following tests should be performed to determine the extent of surface preparation required to ensure a successful coating application.
Test for Curing Compound:
Most concrete has a chemical curing agent applied at the time it is poured. Such chemical curing agents frequently prevent adhesion of coatings. Test for curing compound by applying a muriatic acid solution to bare concrete. If the solution does not react (bubble vigorously), when in contact with the concrete, the presence of a curing com- pound is indicated. Check various areas of the floor. Curing compounds must be either chemically or mechanically removed prior to coating. Generally, acid etching does not remove chemical curing compounds
Test for Grease:
The presence of oil or grease will interfere with coating adhesion. Dark and discolored areas often indicate that grease and/or oil has contaminated the floor. Test for contamination by pouring a small amount of water on the floor. If it beads up, oil and/or grease is present. Another test that can indicate the presence of oil or grease is to press a strip of duct tape firmly onto the surface. If the duct tape does not strongly adhere to the surface, oil and/or grease may be indicated. If grease or oil is present, the floor must be degreased before further surface preparation is performed.
Test for Moisture:
There may be moisture in the concrete, or moisture vapor may be seeping up through it. Test for moisture by taping a 2’x2’ plastic sheet over different areas of the floor. Exam- ine the plastic after 24 hours for signs of moisture. If moisture is present the floor should not be coated until the source of the moisture is determined. Hydrostatic pressure occurs when a body of water, restricted by any structure, is prevented from flowing along its normal path The pressure created by this build of water exerts unpredictable amounts of pressure on the concrete itself and any coating that may be attached. This force has the ability to cause failure in a concrete foundation and potentially a failure in any coating system applied where hydrostatic pressure exists. Because the effects of hydro- static pressure can not be predicted, there exists no guarantee by Diamond Vogel that any coating will be able to withstand the forces capable of causing failure in the concrete substrate.
Test Adhesion of Previous Coatings:
Some coating systems do not require the complete removal of previously applied coatings in order to repaint the floor, but all existing coating that remains that is painted over must be tightly adherent. After required mechanical and chemical cleaning of the surface is accomplished, cut 2”x2”“X” cross-hatches into remaining coatings. Then, apply 6” stripes of duct tape over the X’s, press the duct tape firmly onto the floor, and then quickly pull it off. If large portions of the prior coating come off with the tape, additional surface preparation must be done before recoating. The applicator of the coating is responsible for determining whether the floor will hold a coating or not.
Abrasive blast cleaning may be necessary to completely remove all existing coatings and to provide a new surface profile. Some floors may be impregnated with oils, solvents, or water to such a degree that coating adhesion will be impossible even with abrasive blasting. If the floor has been heavily soiled in the past, it is recommended that a core sample of the concrete be taken to determine the level of contamination. If the core sample indicates contamination into the concrete that cannot be removed by abrasive blasting, the floor will probably never allow a coating to adhere.
Degreasing a Concrete Floor
Dampen the concrete surface and then apply a 1:1 solu- tion of Great Lakes Laboratories’ Extra Muscle and water. Allow to soak for 15 to 20 minutes. Keep the surface wet by adding water while scrubbing the solution over the entire floor with an electric floor scrubber or stiff bristle brush. Rinse floor thoroughly using a power washer with a minimum 1000 psi and a minimum fluid flow of 1 gpm. Final rinse water should be neutral–pH 7. Allow to dry. The color and dullness of the floor should be uniform.
Dark areas indicate the presence of grease/oil, and the floor must be degreased again. Check for invisible grease/ oil in several areas of the floor by applying a 1:1 solution of muriatic acid to the floor. If the acid turns brown or does not react (bubble), grease/oil has penetrated the floor and a repeat degreasing procedure is necessary. Repeat the acid test after subsequent degreasing until all areas tested indicate the floor to be free of grease and oil. After repeat degreasing, rinse the floor by power washing to a neutral pH. Duct tape should adhere tightly to a properly degreased floor. If the tape does not tightly adhere, the presence of grease is indicated and further degreasing is necessary.
Preparing a Concrete Floor By Acid Etching
Sweep the floor clean and dispose of dust. Remove from the floor any contaminant, including oil and grease. Dampen the floor and apply a 1:1 solution of muriatic acid and water through a sprinkling device. The acid should bubble vigorously when applied to the concrete. Coverage should be about one gallon of solution per 100 square feet. Allow reaction between solution and concrete to occur for approximately 3-5 minutes, then follow with a stiff broom or mechanical scrubber to remove surface laitance. Rinse the etched surface with clean water, preferably with a high pressure washer. If use of a pressure washer is not possible, rinse and remove water a minimum of three times to ensure a complete rinse is obtained. Do not let the acid dry out on the floor. Continue power scrubbing while rinsing with clean potable water.
Household ammonia or soda ash may be added in the rinse to help neutralize the acid. Pick up the water. Litmus paper should be used to check the pH of the rinse water. If the rinse water is not pH neutral (pH 7-8) or if there ap- pears to be a film on the floor, additional rinsing is neces- sary. Allow the surface to completely dry, then vacuum again to remove fine particles loosened by the acid-etch. Do not allow unneutralized acid solution to flow into the sewer system or ground.
Preparing a Concrete Floor By Shot Blasting
Sweep the floor clean and dispose of dust. Remove from the floor any contaminant including oil and grease. Shot blast to produce a 3-4 mil profile on the concrete floor. The shot blasting machine must be equipped with a vacuum system to recover shot and to reduce airborne dust and contaminants. After blasting sweep the floor to remove any shot, dust and loose contaminants. Areas that cannot be reached with the blasting machine must be mechanically abraded by handheld devices to remove curing compound and produce a minimum 3-4 mil profile.
Dynamic and Non-Dynamic Cracks
Dynamic cracks or joints greater than 1/4” should be filled with Vulkem #45 Polyurethane sealant after the coating is applied (within three months). De-gloss the coating adjacent to the joint by scuffing with 3M #7447 Scotch- Brite hand pads. Vulkem #45 requires a minimum of 24 hours drying time to become tack free and requires 7 days for a full cure. This product cures by reacting with moisture in the air. Curing can be sped up by misting the sealant with moisture after application, but you must anticipate a period in which you can not drive or walk directly onto the sealant.
Joints should be filled from the deepest point to the surface. In joints over 1/2” sealant depth should be controlled to a maximum of 1/2” with Closed Cell Backer Rod.
Fill all holes, spalled spots, and random non-dynamic cracks with Nu-Klad 114A Epoxy Filler. Body-up compound with silica sand when filling holes over 1/4” in diameter. Areas must be dry and dust free. Apply Nu-Klad 114A Epoxy Filler into depressions with a putty knife and smooth to an aesthetic appearance. 114A will not shrink and cannot easily be sanded once cured. Allow 12-48 hours for cure depending upon temperature.